Step-growth polymerisation (2): production of nylon

Product No: P1172100

Principle

The reaction of sebacoyl chloride with hexamethylenediamine forms Nylon 610®. The two components are dissolved in two solvents of different density which do not mix with one another. For this reason, a reaction can take place only at the contact surface between the two phases. This interfacial polymerisation makes it possible to pull a continuous string from the glass beaker (rope trick). The test can also be carried out without the winding reel pictured here. In that case the nylon thread is simply wound up onto a glass rod.





Materiallist (Excerpt) Product Amount
Sliding weight balance, Kern 150-23, 101 g / 0.01 g 44012-01 1
Sebacoyn dichloride f.synth.25 ml 31833-04 1
Sodium hydroxide, flakes, 500 g 30157-50 1
Hexamethylene diamine 25 g 31367-04 1
Dichloromethane 250 ml 31255-25 1
Denaturated alcohol (spirit for burning), 1000 ml 31150-70 1
Erlenmeyer flask, narrow neck, 100 ml, PN 19 36418-00 1
Phenolphthalein, 0,5% soution in ethanol, 100 ml 31715-10 1
Protecting glasses, clear glass 39316-00 1
Rubber gloves, size 8.5 39323-00 1
Dish, plastic, 150x150x65 mm 33928-00 1
Graduated cylinder 10 ml 36625-00 1
Graduated cylinder 50 ml 36628-00 1
Glass beaker DURAN®, short , 250 ml 36013-00 1
Tweezers,straight,blunt, 130 mm 64610-00 1
Wash bottle, plastic, 500 ml 33931-00 1
Glass rod,boro 3.3,l=200mm, d=5mm 40485-03 1

Literature for this article als follows

Title Product Language
TESS advanced Chemie Handbuch Polymerchemie 01838-01 DEU
TESS advanced Chemistry manual Chemistry of Polymers 01838-02 ENG
TESS advanced Química manual Química de los Polimeros 01838-04 ESP

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Product No: P1172100

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