Determination of the heating values of liquids in a vertical calorimeter

Product No: P1224251

Principle

In general, the combustion of liquids in calorimeters is particularly problematic, because the conditions required for perfect, complete and safe combustion processes are different for practically every liquid. The vertical calorimeter setup used here avoids these difficulties in a simple manner. For burning liquids, a small, easy-to-handle spirit burner with an adjustable wick is used, which makes it possible to burn a variety of liquids (such as alcohols, heating oils, diesel fuel, paraffin, etc). Only highly viscous fluids cannot be burned in this way.
The gases formed during combustion are drawn into the calorimeter insert by means of a water jet pump. In this way, nearly all of the heat energy released during the experiment is delivered to the calorimeter, thereby making it possible to determine the heating capacity of the fluid burned. 




Materiallist (Excerpt) Product Amount
Set of Precision Balance Sartorius CPA 623S and measure software, 230 V 49224-88 1
Glass jacket 02615-00 1
Calorimeter insert f.glass jacket 02615-01 1
Lab jack, 160 x 130 mm 02074-00 1
Retort stand, h 750 mm 37694-00 1
Magnet, d 10mm, l 200mm 06311-00 1
Test tube GL25/8, w.hose connec. 36330-15 1
Water jet pump, plastic 02728-00 1
Spirit burner, adjustable 32154-00 1
Lab thermometer,w.stem,+15..+40C 38057-00 2
Glass tubes,right-angled, 10 36701-59 1
Universal clamp 37715-00 3
Lab protecting glasses with UV filter 39315-00 1
Right angle clamp 37697-00 3
Rubber caps, pack of 20 02615-03 1
Graduated vessel, 1 l, with handle 36640-00 1
Pinchcock, width 15 mm 43631-15 1
Silicone tubing i.d. 7mm 39296-00 1
Funnel, glass, top dia. 55 mm 34457-00 1
Magnetic stirring bar 30 mm, cylindrical 46299-02 1

Literature for this article als follows

Title Product Language
Demo advanced Chemie Handbuch Glasmantel (GLT) 01196-11 DEU
Demo advanced Chemistry Manual Glass Jacket System (GLT) 01196-12 ENG

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Product No: P1224251

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