Tertiary butylhalogenides are saponified in aqueous and aqueous basic solutions according to an SN1 mechanism to tertiary butanol. The kinetics of the reaction can be followed via the temporal consumption of hydroxide ions and evaluated accordingly.
| Materiallist (Excerpt) |
Product |
Amount |
|
Set of Precision Balance Sartorius CPA 623S and measure software, 230 V
|
49224-88
|
1
|
|
Magnetic stirrer MR Hei-Standard
|
35750-93
|
1
|
|
Digital thermometer, NiCr-Ni, -50...+1300°C
|
07050-00
|
1
|
|
Immersion probe NiCr-Ni, steel, -50...400°C
|
13615-03
|
1
|
|
tert.-Butyl chloride, 250 ml
|
30045-25
|
1
|
|
Burette clamp, roller mount.,2pl.
|
37720-00
|
1
|
|
Caustic soda sol.,1.0M 1000 ml
|
48329-70
|
1
|
|
Burette 10ml,strai.stopc.,Schellb
|
47152-01
|
1
|
|
Stopwatch, digital, 1/100 s
|
03071-01
|
1
|
|
Water, distilled 5 l
|
31246-81
|
1
|
|
Pipette dish
|
36589-00
|
1
|
|
Bromothymol blue,indicator 1 g
|
31138-01
|
1
|
|
Acetone, chem.pure 250 ml
|
30004-25
|
1
|
|
Supp.rod stainl.st.,50cm,M10-thr.
|
02022-20
|
1
|
|
Erlenmeyer flask, narrow neck, PN 29
|
36424-00
|
1
|
|
Pipettor
|
36592-00
|
1
|
|
Universal clamp
|
37715-00
|
2
|
|
Crystallizing dish, boro3.3, 1000ml
|
46245-00
|
1
|
|
Pasteur pipettes, 250 pcs
|
36590-00
|
1
|
|
Weighing dishes, square shape, 84 x 84 x 24 mm, 25 pcs.
|
45019-25
|
1
|
|
Volumetric flask 100 ml, IGJ12/21
|
36548-00
|
2
|
|
Volumetric flask 50 ml, IGJ12/21
|
36547-00
|
1
|
|
Right angle clamp
|
37697-00
|
2
|
|
Volumetric pipette, 50 ml
|
36581-00
|
2
|
|
Rubber caps, 10 pcs
|
39275-03
|
1
|
|
Glass beaker DURAN®, tall, 50 ml
|
36001-00
|
1
|
|
Volumetric pipette, 20 ml
|
36579-00
|
1
|
|
Microspoon, steel
|
33393-00
|
1
|
|
Volumetric pipette, 10 ml
|
36578-00
|
2
|
|
Funnel, glass, top dia. 55 mm
|
34457-00
|
1
|
|
Magnetic stirring bar 30 mm, cylindrical
|
46299-02
|
2
|
|
Wash bottle, plastic, 500 ml
|
33931-00
|
1
|
|
Rubber stopper 26/32 , without hole
|
39258-00
|
2
|
|
Rubber stopper, d=9/5mm, w/o hole
|
39250-00
|
1
|
|
Laboratory Experiments Physics, Chemistry, Biology andApplied Sciences, CD-ROM, incl. operating manuals
|
16502-42
|
1
|
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