Product details

Boiling point diagram of a binary mixture

Boiling point diagram of a binary mixture

Item no.: P3030401

Difficulty Expenditure of Time print
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Principle

A boiling point diagram shows the boiling points of a binary mixture as a function of the vapour / liquid equilibrium of the mixture at constant pressure. The boiling points of various mixtures of methanol and chloroform are measured and the composition of the liquid phases are determined using refractometry and a calibration curve.

Benefits

  • Important basic experiment for distillation
  • Excellent for the introduction of refractometry

Tasks

  1. Determine the refractive indices of the pure components and about 10 different mixtures of known composition.
  2. Plot the boiling point diagram of the binary mixtures of methanol and chloroform.

What you can learn about

  • Fundamentals of distillation
  • Equilibrium diagram
  • Chemical potential
  • Activity coefficient
  • Raoult's law

 

Additional necessary

  • Chloroform
Device Name Item no. Qty
Dimroth condenser MAU-26525500 1,00
Erlenmeyer nar.neck.,100ml 46141-00 1,00
Funnel, glass, top dia. 50 mm 34457-00 3,00
Bath for thermostat, makrolon 08487-02 1,00
Water jet pump, plastic 02728-00 1,00
Clamp f.ground joint,plastic,NS19 43614-00 3,00
Laboratory pen, waterproof, black 38711-00 1,00
PHYWE Temperature meter digital, 4-2 13617-93 1,00
Rubber tubing, i.d. 10 mm 39290-00 1,00
Right angle boss-head clamp 37697-00 2,00
Round bottom flask, 250 ml, 2-neck, IGJ 19/26 35843-05 2,00
External circulation set for thermostat Alpha A 08493-02 1,00
Teflon sleeve IGJ 19, 10 pcs 43616-00 1,00
Rubber stopper,d=24/18mm,w/o hole 39256-00 11,00
Pasteur pipettes, 250 pcs 36590-00 1,00
Glycerol, 250 ml 30084-25 1,00
Heating mantle f. roundbottom flask, 250ml 49542-93 1,00
Hose clamp for 5-12 mm diameter 40997-00 14,00
Universal clamp 37715-00 2,00
Abbe refractometer 35912-00 1,00
Immersion thermostat Alpha A, 230 V 08493-93 1,00
Sheath Thermocouple, NiCr-Ni, Type K, -40°C ... +1000°C 13615-06 1,00
Beaker, 100 ml, high-form 46026-00 2,00
Rubber caps, 10 pcs 39275-03 1,00
Boiling beads, 200 g 36937-20 1,00
Power regulator 32288-93 1,00
Clamp for heating mantle 49557-01 1,00
Stopper, IGJ 19/26,glass,clear 41252-10 1,00
Burette clamp, roller mount., 2 pl. 37720-00 1,00
Column head, with stopcock, ST 19/26 35919-01 1,00
Protective sleeves f.temp.probe,2 11762-05 1,00
Rubber tubing, i.d. 6 mm 39282-00 5,00
Retort stand, h = 750 mm 37694-00 2,00
Universal power supply600mA 3V/ 4,5V/ 5V/ 6V/ 7,5V/ 9V/ 12V incl. 8 adaptors 11078-99 1,00
Tubing connector, ID 6-10mm 47516-01 2,00
Document     Filesize
p3030401e.pdf Experiment guide, English 331.54 KB

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