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Technical data


XR 4.0 X-ray material upgrade set

Article no: 09165-88

Function and Applications

Upgrade set as an extension of the XR 4.0 X-ray unit.

This set is particularly suitable for the qualitative and quantitative X-ray fluorescence spectroscopy of metallic samples in physics and material science (non-destructive testing).

The set covers the following experiments and topics:

  • Various different types of samples can be analysed: powders, solids, and liquids
  • Material analyses of pure metals and multi-component alloys
  • Moseley's laws energy-dispersive Bragg structure analysis
  • Determination of the lattice constant of monocrystals
  • Duane-Hunt's law of displacement
  • X-ray fluorescence analysis for layer thickness determination
  • Characteristics and the special resolving power of an X-ray energy detector

Benefits

  • Immediate measurements possible because energy detector does not require warm-up
  • Measurement data can be viewed in real-time as soon as x-ray tube is switched on
  • In combination with the XR 4.0 X-ray multi-channel analyser, the entire X-ray energy spectrum (2-35 keV) of the analysed materials can be determined.
  • The set includes a sensitive XR 4.0 X-ray energy detector with a resolution of FWHM < 400 eV, rate independent up to 20 kcps.
  • The XR 4.0 X-ray energy detector is mounted directly and easily onto the XR 4.0 X-ray goniometer (09057-10) of the XR 4.0 X-ray unit.
  • Direct connection of the XR 4.0 X-ray energy detector via the internal and external socket panel to the multichannel analyser that also supplies the supply voltage.

Equipment and Technical Data

The set includes the following components:

  • XR 4.0 X-ray energy detector
  • Multi-channel analyser
  • Software for the multi-channel analyser
  • XR 4.0 X-ray set of chemicals for edge absorption
  • XR 4.0 X-ray lithium fluoride (LiF) monocrystal in a holder
  • XR 4.0 X-ray universal crystal holder for the X-ray unit
  • XR 4.0 X-ray sample holder for powder samples
  • XR 4.0 X-ray diaphragm tube with Zr foil
  • additional accessories

Additionally required are an X-ray tube (09057-51, 09057-61, 09057-71, 09057-81) and a goniometer (09057-10).

Include chemicals needed for experiments (09056-04)

 

 

 

Scope of delivery

PHYWE Multichannel Analyser (MCA) 13727-99 1
XR 4.0 X-ray energy detector (XRED) 09058-30 1
XR 4.0 X-ray LiF crystal, mounted 09056-05 1
XR 4.0 X-ray Universal crystal holder for X-ray unit 09058-02 1
XR 4.0 X-ray specimen set of 6 metals for X-ray fluorescence 09058-31 1
XR 4.0 X-ray Specimen set alloys for fluorescence, set of 5 09058-33 1
XR 4.0 X-ray specimen set metals for fluorescence, set of 4 09058-34 1
XR 4.0 X-ray Compton attachment 09057-04 1
XR 4.0 X-ray sample holder for powder samples (diffractometry) 09058-09 1
XR 4.0 X-ray Diaphragm tube d = 1 mm 09057-01 1
XR 4.0 X-ray Diaphragm tube d = 2 mm 09057-02 1
XR 4.0 X-ray Diaphragm tube d = 5 mm 09057-03 1
Ores collection, 40 ores 39782-00 1
Compact Balance, OHAUS NV 422, 420 g / 0.01 g 49248-93 1
Macro-cuvettes, PS, 4ml,100 pcs 35663-10 1
Graduated pipettes, various sizes 36600-00 3
Pipettor 36592-00 1
Snap-cap vials,d=28mm,h=75mm,10p. 33622-03 1
Beakers, Boro, low form, various sizes 46054-00 3
Beaker, 100 ml, plastic (PP) 36011-01 1
Spatula, powder, steel, l=150mm 47560-00 1
Spoon + spatula, steel, l=120mm 46949-00 1
Glass rod,boro 3.3,l=200mm, d=4mm 40485-02 2
Crucible tongs, 200 mm, stainless steel 33600-00 1
Evaporating dish, porcelain, various sizes 32514-00 1
measure Software multi channel analyser 14452-61 1

Necessary accessories

XR 4.0 X-ray goniometer 09057-10
XR4 X-ray Plug-in Cu tube 09057-51

PHYWE Systeme GmbH & Co. KG
Robert-Bosch-Breite 10 – 37079 Göttingen – Germany
www.phywe.com