Principle
A polycrystalline zirconium foil is irradiated with X-rays. The resulting Debye-Scherrer reflections are photographed and then evaluated.
Tasks
- Take Debye-Scherrer photographs of the zirconium sample.
- Evaluate the Debye-Scherrer rings and assign them to the corresponding lattice planes.
- Determine the lattice constants of the sample material.
- Determine the number of atoms in a unit cell of the sample.
Learning objectives
- Crystal lattices
- crystal systems
- reciprocal lattice
- Miller indices
- structure amplitude
- atomic form factor
- Bragg scattering
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p2541501d .pdf
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